Intensification of technological processes in tin production

Научное издание / монография

Выпущено ООО Издательский дом «БИБЛИО-ГЛОБУС»

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Рецензенты:
Олейникова Наталья Васильевна - профессор кафедры металлургии цветных металлов Института цветных металлов и материаловедения ФГОАУ ВО «Сибирский федеральный университет», доктор технических наук
Кокоева Наталья Борисовна - кандидат технических наук, доцент кафедры металлургии цветных металлов и автоматизации металлургических процессов ФГБОУ ВО СКГМИ (ГТУ)

Abstract:
The author's monograph summarizes the practice of experimental research on the intensification of technological processing of tin production in order to create promising technologies and solve private bottlenecks. Special attention is paid to the intensification of the purification of concentrates from difficult-to-remove impurities during their melting and refining. For this purpose, a semi-industrial vibration apparatus for countercurrent leaching of concentrates from iron, bismuth, and tungsten with washing and dewatering of the product has been developed. In order to stabilize the purification of concentrates before melting, work was carried out to intensify the process of sulfate-chlorinating roasting from iron, sulfur, and arsenic impurities. The technology and apparatus for roasting concentrates with ammonium chloride with the regeneration of the reagent in circulation and the conversion of sulfur into soluble iron sulfate have been developed. However, the importance of mastering these works has disappeared due to the success of the development of centrifugal and vacuum refining of tin. Research on roasting technology continued in the direction of processing of dump sulfide tailings. The result of the work on the chloride-sulfiding roasting of sulfide tailings was the use of the method in the processing of current difficult-to-process industrial products with the release of non-toxic arsenic sulfide and tin stub for fusing. Special attention is paid to the search for selective low-temperature reduction of tin concentrate. The results of a study jointly with the institutes of the SB RAS on the recovery of concentrate by abrasion, under the pressure of an explosion, under the influence of an accelerator electron beam are presented. The work on the intensification of the processes of electric melting and fusing for the processing of certain types of raw materials and the complex extraction of tantalum and tungsten is summarized.

Keywords: leaching, vibration, ultrasound, roasting, reduction, accelerated electrons, electric melting, tantalum, tungsten, fusing.

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84.2. Pat RF No. 2037759 -Fluidized bed furnace for firing materials - Nesterov P.V., Dauletbakov T.S., Dyakov V.E., Koryukov Yu.S., Dugelny A.P., Kostelov V.V.; Novosibirsk Tin Combine, Russian concern "Norilsk Nickel", Institute "Gipronikel"\\ Ipc F27b15/00; Application No. 4717978, dated 05/16/1989; Publ.. 19.6.95. BiNo.17-95-196.
85.2. Nesterov P.V., Dauletbakov T.S., Isakova R.A., Soloviev B.A., Dyakov V.E. Fractional condensation of tin, lead, bismuth and arsenic compounds on a vacuum-fluidized bed installation.- \\ Technology of processing tin-containing raw materials, Collection of scientific papers, Novosibirsk, Tsniiolovo, 1985, pp.72-75.
86.2. Pat RF No. 1351120 Method of processing poor sulfide-arsenic tin raw materials; Dyakov V.E., Soloviev B.A., Selivanov I.M., Koryukov Y.S., Dugelny A.P., Nesterov P.V., \\ From 22 To 7/00; application 4024494 from 12/24/85.; publ.27.06.12; №18-12- c447.
87.2. Pat RF No. 2529349 Method of processing tin-containing sulfide tailings and firing apparatus for its implementation; Dyakov V.E \\ C22B 1/04; Application No.2013113993 dated 28.03.2013; pub pat 20.05.15 No. 14.
88.2. Pat RF No. 2602204 Method of processing tin-containing sulfide tailings and firing apparatus for its implementation; Dyakov V.E.\\ C22B 25/02; No. 2015128118 dated 10.07.2015; Publ. 10.11.2016 Byul. No. 31.
89.2.Lebedev I.S., Nekrasov V.I. Arzamassev Yu.S., Evdokimov V.I., Semenov A.E., Koryukov Yu.S., Dyakov V.E. -Physico-chemical bases of dearsenizing firing of industrial products of finishing tin concentrates with natural forms of sulfide-arsenic minerals \\ Scientific works of TSNIIOLOVO, Novosibirsk, 1983, c39-47.
90.2. Pat RFNo. 1064637 Method of processing poor tin raw materials - Semenov A.E., Lebedev I.S., Koryukov Yu.S., Evdokimov V.I., Dyakov V.E., Selivanov I.M., Sukhoi G.N., Nekrasov V.I., Bogdanov V.A., Arzamassev Yu.S., Nesmelov V.N., Sizykh N..G., Tsniiolovo, NOC \\ Application No. 2984074 dated 09/23/80. Publ. 10.07.12. No.19-12-p.509.
91.2.Arzamassev Yu.S., Lebedev I.S., Nekrasov V.I. -Dearsenizing roasting of sulfide-arsenic products\\ Scientific works of Tsniiolovo, 1982, c64-68.
92.2. Varnek V. A., Dyakov V. E., Koryukov Yu. S.- Research by the JAGR method of dump tin production intermediates in the processes of their firing \\ zh. Complex use of mineral raw materials, 1986, No. 6, pp.35-37.
93.2. Pat RFNo. 1061486 Method of firing fine tin raw materials -Semenov A.E., Lebedev I.S., Dyakov V.E., Koryukov Y.S., Nekrasov V.I., Mukhin N.A., Koryukova L.M., Galeev I.K., Alekseeva N.K., Soloviev B.A., Sivolob V.V., Arzamassev Y.S., Nebaba G.M., Fomina L.S.; NOC, Tsniiolovo\\ application No. 3433304 dated 15.02.82; Publ. 10.07.2012. No. 19-12-c509.
94.2. Nekrasov V.I., Lebedev I.S., Dyakov V. E., Alekseeva N. K., Babievskaya I. 3.- Study and improvement of the technology of firing tin-containing raw materials in multi-pod furnaces\\ Collection of scientific works of TSNIIOLOVO "Tin production technology, Novosibirsk, 1986, pp.48-53.
95.3. Avvakumov E.G., Dyakov V.E., Strugova L.I., Boldyrev V.V., Koryukov Yu.S., Devyatova L.B. Mechanical activation of solid-phase reactions. Solid-phase reduction of cassiterite, \\Izvestiya SB AS USSR, ser.chem.n, . 1974, 2, 26-28,
96.3.Auth of the Holy Russian Federation No. 453934. Method of processing tin concentrates - Avakumov E.G., Dyakov V.E., Boldyrev V.V., Koryukov Y.S., Devyatova L.B., Strugova L.I., IHKG SB RAS, NOC \\C22b25\02; application No.1651654 of 27.04.71; publ 16.01.76.; Bi35-75-178.
97.3. Avvakumov E.Gorenje, Dyakov V.E., Matytsin A.I., Staver A.M. Solid-phase reduction of SnO2 under shock compression and mechanical activation, Physics of Combustion and Explosion, 1975, 6, 922-927.
98.3.Solid-phase reduction of tin dioxide under shock compression and activation in a grinding apparatus - Matytsin A.I., Avvakumov E.G., Dyakov V.E., Staver A.M. - Abstracts of the Fifth All-Union Symposium on Mechanical Emission and Mechanochemistry of Solids, Tallinn, 1975, s77-78.
99.3. Matytsin A.I., Avvakumov E.G., Deribas A.A., Dyakov V.E., Staver A.M. - Features of chemical reactions under shock loading of powder mixtures Collection "The effect of high pressures on matter", Kiev, Institute of Problems of Materials Science of the National Academy of Sciences of Ukraine 1976, s59-62.
100.3. Metallurgist's Handbook on non-ferrous metals, t2, ed. Murach N.N., M, 1947, 781c.
101.3. Koryukov Yu S., Suturin S. N. -Recovery of tin concentrates with a mixture of hydrogen and carbon monoxide.- \\ Non-ferrous metallurgy, M, 1969, No.8,s48-49.
102.3. Pat RF No. 1794098 Method of tin production - Kostelov V.V., Baymakov A.Yu., Koryukov Yu.S., Dyakov V.E., Dugelny A.P., Murkin V.A., State Design and Research Institute of Nickel-Cobalt industry and Novosibirsk Tin Combine\\ C22b5\00; application No. 4943215 of 30.04.91; publ., 7.02.93 Bi No.5-93-208.
103.3. Pat RF No. 1794102 Method of obtaining tin from tin-containing materials - Kostelov V.V., Baymakov A.Yu.; Murkin V.A., Dugelny A.P., Koryukov Yu.S., Dyakov V.E., "Gipronikel" and NOC.\\ From 22b25/02; application No. 4379387 dated 10.12.87; publ. 07.02.93. Bi. No.5-93-209.
104.3. Pat RFNo. 794237 Mine reactor -Kostelov V.V., Baymakov A.Yu., Koryukov Yu.S., Dugelny A.P., Dyakov V.E., Murkin V.A., Borisov O.G., Gnedin I.I.; Gipronickel, and NOC \\ F27b4/00; application No. 4947942 dated 24.06.91; publ. 07.02.93, BI No.5-93-c232.
105.3. Pat RF No. 2061722 Method of obtaining metallic tin- Dugelny A.P., Koryukov Y.S., Dyakov V.E., Baymakov A.Yu., Derevenskiy B.P., Klementyev V.V., Rivlin A.L., Yushkevich G.N.- \\ C22b25\02; application No.93008706 of 15,02,93; publ. 10.06.96 BiNo.16-96-217.
106.3. Author of the Holy USSR No.720838 Linear ion accelerator-Auslander V. L., Baranov I. A., Lazarev V. N., Panfilov A.D., Smirnov B.M., Trofimenko S. M., Shilov V.P., Eismont V.P. \\M.cl.H05 h9/00; Application No. 2628375 dated 06/13/78, Pub. 05.03.80. Bi No. 9.
107.3. Komlev A. S. Electron accelerators for radiation-thermal technology for obtaining ferrite ceramics\\ Tauride Scientific Observer, 2016, No. 12 (17), Part 1, c142-145.; www.tavr.science http://tavr.science/stat/2016/12/72-Komlev.pdf .
108.3. Pat RF No. 1700071 Method of metal recovery from ore concentrate - Bochkarev G.R., Voronin A.P., Dugelny A.P., Dyakov V.E., Rostovtsev V.I., Rusakov S.,V.; IGD SB RAS;\\ C22B5/02; Application No. 4109560 dated 08/29/1986 opis publ 23.12.1991;. Bi 91-47-106.
109.3. Rusakov C.B., Auslander V.L., Bochkarev I.G., Voronin A.P. Gribkov O.S., Lyakhov N.Z., Modestov A.N., Polyakov V.A. Reduction of metal oxides by hydrogen in a beam of accelerated electrons // Izvestiya SB AN USSR. 1987., Ser chem. nauk. - Vol.1. - pp. 36-41.
110.3.Pat EP WO8902480 -Method of metal recovery from metal-containing material; Bochkarev G.R., Voronin A.P., Dugelny A.P., Dyakov V.E., Rostovtsev V.I., Rusakov S.V., Adigamov B.Ya., Weigelt Yu.P., Weiss M.E., Voitkovsky Yu.B., Goryagin E.P., Gribov O.S., Kurbatov V.P., Miroshnichenko I.I., Polyakov V.A., Taletsky Yu.V., Shalatsky S.V., Auslender V.L., Boldyrev V.V., Krainin S.M., Lyakhov N.Z., Solovetsky Yu.,I., Shemyakin E.I.\\Cl.C22b5\02; International application (appl) PCT/SU87\00103 of 17.09.87, Publ. 23.03.89; 30pp.
111.3. German Patent No. 3791011. Verfahren zur Metallgewinnung metallhaltigen Stoffen / G.R. Bockarev, A.P. Voronin, A.P. Dugehiyj, V.E. Djakov, V.l. Rostovcen, S.V. Rusakov, B.J. Adigamov, J.P. Veigelt, M.E. Veis, J.B. Voitkovskyj, E.P. Gorjagin, O.S. Gribkov, V.P. Kurbatov, I.l. Mirosnicenko, V.A. Poljakov, J.V. Taleckyj, S.V. Salackyj, V.L. Auslender,
V.V., S.M. Kreinin, N.Z. Ljachov, J.I. Soloveckyj, E.I. Semjakin. München,\\ MKI5 C22 B5/02; 07/19/90. 1990.
112.3. Swedish Patent No. 463877 Forfarande für reduktion av metal ur metallhalting material/ G.R. Bochkarev, A.P. Voronin, A.P. Dugelny, V.E. Dyakov, V.L. Rostovtsev, S.V. Rusakov, J.P. Veigelt, M.E. Veis, V.A. Polyakov, V.L. Auslender, V.V. Boidyrev, N.Z. Lyakhov, O.S. Gribkov, B.Y. Adigamov, E.P. Goryagin, 1.1. Miroshnichenko, J.V. Taletsky, S.V. Shalatsky, J.I. Solovetsky, .B. Voitkovsky, V.P. Kurbatov, S.M. Kreinin, E.I. Shemyakin, SVERIGE, MKI5 C22 B5/02; 4.02 91.1991.
113.3. Abramson I.G., Shlionsky Yu.S. Using high-energy electron beams to remove harmful oxides from exhaust gases // Cement and its application, 2005. No. 1, pp. 75-76.
114.3. Varnek V.A., Chernikova L.V., Mazalov L.P., Dyakov V.E., Koryukov Yu.S. Method of nuclear gamma-resonance-a new method of control of tin production processes, 1988, Vses. chem. total., 43str.
115.3. Rostovtsev V.I., - Development of highly effective technologies of electrochemical, radiation and radiation-thermal effects on ore preparation and enrichment of resistant mineral raw materials, \\IGD Sb RAS. Kulagin Readings: XI International Scientific and Practical Conference. - Chita. ZabGU, 2011. page 82(263c).
116.3. Technology for obtaining wear-resistant coatings on titanium alloys using an industrial electron accelerator- ELV-6.- Lenivtseva O.G., Lazurenko D.V., Samoylenko V.V. \\ "Innovative technologies and economics in mechanical engineering", V International Scientific and Practical Conference, 2014, pp. 295-297.
117.3. Science of Siberia-50 (2236) December 24, 1999; https://raen.info/activities/registracija-nauchnyh-otkrytii/spisok-otkrytii111-javlenie-radiacionno-termicheskoi-aktivacii-tverdofaznyh-himicheskih-reakcii-v-neorganicheskih-sistemah.html.
118.4.Author of the Holy USSR No. 540929- A method for processing zinc-containing tin dust; Dyakov V.E, Rodnin Y.R., Makarov G.S., Koryukov Y.S., Novosibirsk Tin Combine \\ C22b7/02; Application No. 2194730 dated 11/27/1975; Publ. 12/30/1976, Bi No. 48-76-83.
119.4.Auth of the Holy USSR No. 609336 Method of processing materials containing tin, indium and zinc; Dyakov V.E., Semenov A.E., Koryukova L.M.; Novosibirsk Tin Combine\\C22b7/02; Application No.2304244ot 29.12.1975; Publ. 10.03.2012 BiNo. 7.
120.4. Auth of the Holy USSR No. 917546 Method of extraction india from dust; Alekseev S.A., Dyakov V.E., Alekseeva N.K., Chereshnev S.R., Mukhin N.A., Zavozin N.I.; Central Research Institute of Tin Industry, Novosibirsk Tin Combine\\ C22b7/02; Application: 2990840 dated 03.10.1980; Publ. 27.06.2011; BiNo. 18-11-c1082.
121.4.Auth of the Holy USSR No. 606365 - A method of processing tin-lead materials; Dyakov V.E., Galeev I.K., Alekseeva N.K.; Novosibirsk Tin Combine\\ With 22b7/02; Application No. 2434285 of 25.12.76; publ. 07.06.86. Byul. No. 21.
122.4. Auth of the Holy USSR No. 478524- A method for processing copper-antimony tin-containing tin refining waste; Kozhnova R. V., Dyakov V. E., Levchenko M. P., Stepanov G. I., Lelyuk V. G. \\ From 22B 7/00; Application No. 199666 of 26.02.74; Publ. 28.02.78. Bi No. 8 -1978-246 .
123.4.Author of the Holy USSR No. 896920 Method of smelting tin from tin-containing materials; Dugelny A.P., Dyakov V.E., Koryukov Y.S., Semenov A.E., Suturin S.N., Dvurechenskaya E.D., Novopashin A.I., Shved G.E., Cherkassky R.I., Kuvshigov V.A., B.V.Klimantov; Novosibirsk tin mill\\ From 22 b 25/02; Application No. 2974172 dated 14.08.80; publ. 10.03.12. BiNo.7-2012-380.
124.4.Auth.sv.USSR No. 790808, A method for processing tin materials.-Suturin S.N., Dyakov V.E., Dolgov A.V., Cherkassky R.I., Klimantov B.V., Kuvshinov V.A., Litovchenko A.P., Kasharnov N.P., Sadykov Z.G., Sulakov V.P., Goldman A.G. -Magnitogorsk Metallurgical Combine, Institute of Hydrodynamics SB AS USSR, Novosibirsk Tin combine\\ From 22 b 25/02; -application No. 2803778, dated 02.08.1979; Pub 10.11.2011, Bi 31-11-c1126.
125.4. Dyakov V.E.- Regeneration of non–ferrous metals from waste by centrifugal filtration\\ monograph, M. BIBLIO-GLOBUS, 2018. 116 p.
126.4.Dyakov V.E.-Centrifugal filtration of molten tin and lead: monograph. M. Publishing House of the Academy of Natural Sciences, 2019 140 p
. 127.4. Author of the Holy USSR No. 653923 Method of processing tin-containing materials; Dyakov V.E., Suturin S.N., Kozhnova R.V., Koryukov Yu.S.; Novosibirsk Tin Combine\\ C22b25/02; application No. 2523114 of 29.08.77; Publ. 10.03.2012; BI No. 7-2012.
128.4. Auth of the Holy USSR No. 788768 - A method for processing arsenic tin refining residues; Makarov G.S., Dyakov V.E., Nesmelov V.N., Koryukova L.M., Alekseeva N.K. Novosibirsk Tin Combine\\ With 22b25/02; 2779169 of 13.06.79; publ. 07.10.92.Byul. No. 37.
129.4.Author of the Holy USSR No. 1457413- Method of tin production; Kleshchenko I.N., Rozlovsky A.A., Mikhalev V.V., Dyakov V.E., Postnikov V.A., Alekseeva N.K., Dzindzeleta V.K., Dugelny A.P., Koryukov Yu.S.\\ C22b25\02; Application No. 4256642 from 04.06.87; publ. 10.07.12 No. 19-12-509.
130.4.Auth of the Holy USSR No. 1420051 Reducing mixture for tin smelting. Postnikov V.A., Dyakov V.E., Sizykh N.G., Mikhalev V.V., Rozlovsky A.A., Dugelny A.P., Alekseeva N.K., Koryukov Yu.S., Kleshchenko I.N., Mukhin V.B.\\ From 22 To 25/00; 4193534 from 12.02.87; Publ. 30.08.88. ByulNo. 32-88-107.
131.4. Postnikov V.A., Dyakov V.E., Semenov A.E., Alekseeva N.K., Shamina O.M. The use of lignin in the melting of tin-containing raw materials\\ Non-ferrous metals, 1989, №1, 54-56.
132.4. Chudakov M.I. Industrial use of lignin \\ M.: Lesn. prom-t, 1983. 200 p.
133.4. Varnek V.A., Dyakov V.E., Investigation by the JAGR method of silicate forms of tin and iron in tin production slags, \\Izv. vuz. Tsv.metallurgy, 1997, No. 4, pp.8-13.
134.4.Auth. USSR No. 1319585 Furnace for melting oxidized tin concentrates; Koryukov Yu.S., Suturin S.N., Tokarev V.S., Feshchenko P.M., Dyakov V.E., Sizykh N.G., Selivanov I.M., Golubeva A.N., NOC\\C22b25\02; application No. 3589679 of 02.03.83.; publ. 27.06.12. No. 18-2012-c447.
135.4. Auth of the Holy USSR No. 851988 Method of processing tin concentrates containing tantalum; Galeev I.K., Chereshnev S.R., Kartashova L.Ya., Dyakov V.E. NOK;\\C22b34/36;application No.2933049 of 30.04.1980; Publ. 10.03.2012 Bul. No. 7.
136.4.Auth of the Holy USSR No. 1061485- Method processing of tin concentrates containing tantalum - Galeev I.K., Dyakov V.E., Lebedev I.S., Bogdanov V.A., Shemyakin V.A., Feshchenko P.M., Makarov G.S., Rodnin Yu.R.; NOC, Gidrotsvetmet,\\ C22b34/36; Application: 3409633 dated 21.01.1982; Pub 10.07.2012 Byul. No. 19.
137.4. Author of the Holy USSR No. 1195661 Method of processing tin concentrates containing valuable components; Galeev I.K., Dyakov V.E., Ustinov V.V., Nikitina V.D., Zavozin N.I., Novosibirsk Tin Combine\\C22b34/36;application No. 3568402 dated 12/27/82;publ.10.07.12; No.19-12-509.
138.4. Author of the Holy USSR No. 1243374 Method of extraction of tantalum and tungsten; Galeev I.K., Dyakov V.E., Ustinov V.V., Zavozin N.I., Nikitina V.D., Chereshneva E.M.; Novosibirsk Tin Combine \\ C22b34/36; application No. 3591902 dated 03.03.1983; Publ 10.07.2012; Byul. No. 19.
139.4. Author of the Holy USSR No. 676009-Method of processing tungsten-containing tin concentrates - Rodnin Yu.R., Makarov G.S., Semenov A.E., Shemyakin V.A., Galeev I.K., Dyakov V.E.;NOC;\\ C22b34/36 Application No.2554724 of 12/16/1977 Publ. 10.03.2012 Byul. No. 7;
140.4.Author of the Holy USSR No. 1226855- Method of extracting tungsten from tin concentrates; Dyakov V.E., Koryukov Y.S., Rodnin Y.R., Galeeva A.V., Kisileva M.P., Alekseeva N.K., Gorodetsky V.D., Zavozin N.I.;\\C22b34/36;Application: 3672820 dated 14.12.1983; Publ 27.05.2012; BiNo.15-2012-c467.
141.4.Varnek V.A., Dyakov V.E., Taskaeva E.L., Zhuzhgov E.L. Investigation by the JAGR method of non-silicate iron in the slag of tin production forms, Izv.universities.Tsv.metallurgy, 1997, No.6,15-19, 8G141-m98, rzh61-98.18L58.
142.4.Auth. USSR No. 1317951- Method of processing tungsten-containing tin concentrates - Mikhalev V.V., Chereshnev S.R., Dyakov V.E., Rodnin Y.R., Dugelny A.P., Galeev I.K., Litvinov N.G., Alekseeva N.K. NOC;\\ C22B 34/36; Application No.3920321 dated 02.07.1985; Publ. 27.04.2013 Byul. No. 12.
143.4. Varnek V.A., Dyakov V.E., Asanov I.P., Lisoivan V.I. On the nature of the presence of tungsten in tin production slags and products of their processing, Izv.universities.Tsv.metallurgy, 1998, No.2,c16-20.
144.4.Author of the Holy USSR No. 1567539 Binder - Khmelenko T.V., Varnek V.A., Dyakov V.E.,SKTB of Industrial Ecology of Siberia at the Kuzbass Polytechnic Institute \\ application No. 4369244 of 25.01.88 publ. 30.05.90 Bi20-90-93.
145.4. Auth sv USSRNo.563018 Method of processing fine tin-containing materials; Rodnin Y.R., Makarov G.S., Dyakov V.E., Bogdanov V.A.; Novosibirsk Tin Combine\\ C22B25/02; Application No. 2195585 of 12.11.1975; Publ. 23.12.1981 BiNo.47-81.
146.4. Auth sv USSR No. 637443- Method processing of fine tin-containing materials -Makarov G. S., Rodnin Y. R., Dyakov V. E., Ustinov V. V., Bogdanov V. A.; Novosibirsk Tin Combine\\ M.Kl.3 From 22 To 25/02; Announced 26.01.77 from 2447039 Publ. 23.12.81. Bi No. 47-81-308.
147.4. Auth. sv.RF No.658900 -Method of processing tin-containing sludge - Dyakov V.E., Suturin S.N., Alekseeva N.K. \\ From 22 To 25/06; application No. 2544497 of 11.10.77; publ. 23.12.81; BiNo. 47-81-c308.
148.4. Auth. sv. USSR No. 1064637 Method of processing poor tin raw materials - Semenov A.E., Lebedev I.S., Koryukov Yu.S., Evdokimov V.I., Dyakov V.E., Selivanov I.M., Sukhoi G.N., Nekrasov V.I., Bogdanov V.A., Arzamassev Yu.S., Nesmelov V.N., Sizykh N.G., Tsniiolovo, NOK \\ Application No. 2984074 dated 09/23/80. Publ. 10.07.12. No. 19-12-p.509.
149.4. Author of the Holy USSR No. 1316259 -Method of processing poor ferrous-tin concentrates -Mikhalev V.V. Dyakov V.E., Rodnin Yu.R., Alekseeva N.K., Kleshchenko T.P., Koryukov Yu.S., Dugelny A.P., Sizykh N.G., Litvinov N.G., Bogdanov V.A.; NOC \\ With 22b25/02; Application No.3881038 of 09.04.85; publ. 27.04.13 Bi No.12.
13.603. 150.4. Varnek V.A., Sokolov V.V., Dyakov V.E.- On the valence-coordination state of iron atoms in tin production slags, \\ Izv.vuz. Tsv.metallurgy, 1997, no.3, pp.10-15.
151.4. Author of the Holy USSR No. 1461011 Method of processing fine tin-containing materials by fusing; Dyakov V.E., Rozlovsky A.A., Kleshchenko I.N., Mikhalev V.V., Bobryshev P.P., Dugelny A.P.\\ From 22 b25/02; Application: No.4284173 of 14.07.87; Publ. 27.06.2012 Byul. No. 18.
152.4.Author of the Holy USSR No. 1636465 Method of tinning waste recycling - Dyakov V.E., Suturin S.N., Koryukov Yu.S., Dalbeev G.V.\\ With 22b25/02; application No. 4488784 of 11.08.89. publ. 23.03.91 Bi No. 11-91-c83.
153.4.Author of the Holy USSR No. 1702701-Method of fusing iron-containing tin materials; Dyakov V.E.; Mikhalev V.V.; Bobryshev P.P.; Kleshchenko I.N.; Rozlovsky A.A.; Novopashin A.I.; Dugelny A.P. \\ application No. 4466292 of 26.07.88. publ. 27.04.13 Bi No. 12-13-603.
154.4. Dyakov V.E.; Fundamentals of centrifugal filtration of zinc waste melts by a submersible filter: monograph. – M.: Publishing House of the Academy of Nature of Knowledge, 2019. – 102 p.
155.4. Author of the Holy USSR No. 1374801 Method of fusing tin-containing slags -Mikhalev V.V., Makarov G.S. Dyakov V.E. Dugelny A.P. Rozlovsky A.A., Rodnin Yu.R., Kleshchenko I.N., Varnek V.A. \\ With 22b25/02; application No. 4031150 of 3.03.86. 27.06.12 No. 18-12-S.447.
156.4. Varnek V.A.,Chernikova L.V.,Kazakova V.I., Dyakov V.E.,Koryukov Yu.S., Study of the phase composition of tin production slags, Non-ferrous metals. 1989, No. 11, pp.43-46.
157.4. Varnek V.A.,Chernikova L.V., Dyakov V.E., Koryukov Yu.S., Kleshchenko I.N. Investigation by the JAGR method of tin-containing slags in the process of fusing, \\zh. Non-ferrous metals, 1989, No.12, pp.35-37.
158.4.Varnek V.A,Chernikova L.V, Kazakova V.I. Dyakov V.E – Gamma resonance and chemical analysis of tin production slags, \\zh.Factory Laboratory, 1990, T56, No. 6, pp.43-46.
159.4. Varnek V.A., Sokolov V.V., Dyakov V.E -The effect of heat treatment on the state of tin in slags,\\ Izv.vuz. Tsv.metallurgy, 1999, No. 4, pp.13-19.
160.4. Author of the Holy USSR No. 1603789 Method of fuming tin-containing slags; Kleshchenko I.N., Dyakov V.E., Rozlovsky A.A., Bobryshev P.P., Kuliyev G.O., Mikhalev V.V., Budanov A.M., Petukhova E.N., Konenkina M.V., Dyakova O.V.; Novosibirsk Tin Combine\\ With 22b25/02; Application No. 4639742 of 19.01.89; publ. 27.06.12.; No. 18-12-447.
161.4. Auth. USSR No. 1711497 Method of extracting tin from slag-Kudenkov V.M., Zykus M.Yu., Bystrov V.P., Dyakov V.E., Dugelny A.P., Koryukov Yu.S., NOC \\ With 22b25/02; application No. 4807524 of 02/20/90; publ. 27.04.13 Bi No. 12.13.603.

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